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Microscale synthesis of UO2Cl2(OPPh3)2 - ResearchGate

Chemistry-major freshmen students as individuals, a group ofone student, worked this AuNPs experiment at a microscale levelfor a three-hour laboratory sessions. The students were firstintroduced to experimental process, content background, especiallyin the synthesis and characterization of AuNPs, and concepts ofmicroscale chemistry and green chemistry. The students then manipulatedexperimental procedures and wrote their own reports and learningfeedback. By the way, the synthesis of AuNPs (excluding the characterization)at a microscale level had been performed within 40 minutes inan event that a class of high-school students visited the chemistryof department in our university. All of the students were a firstexperience in the synthesis of AuNPs. Valuably, they can successto synthesize colloidal AuNPs and most of the students had positiveresponses for the synthesis. Examples of the students' feedbackare as follows: ""and "

Microscale Organic Laboratory with Multistep and Multiscale Syntheses, 6th Edition

Green chemistry: The twelve Principles of Green Chemistrywere originally published by current assistant administrator PaulAnastas of United States Environmental Protection Agency and JohnWarner []. The twelve principlesare: prevention, atom economy, less hazardous chemical syntheses,designing safer chemicals, safer solvents and auxiliaries, designfor energy efficiency, use of renewable feedstocks, reduce derivatives,catalysis, design for degradation, real-time analysis for pollutionprevention, and inherently safer chemistry for accident prevention[]. Our experiment developedat a microscale level attempted to respond to green chemistryfor undergraduate laboratory instruction.

24/11/2017 · Request (PDF) | Microscale synthesis..

KW - microscale synthesis

Research areas include scalable synthesis of nanomedicines,microfluidic diagnostics, high throughput biomarker analysis, and microscale platforms for probing lipid membranes and ion channels.

76, Issue 2, p.237The synthesis of tetraphenylporphyrin, H2[TPP], andpara-substituted tetraphenylporphyrins,H2[(p-X)4TPP], where X = CN, CH3, andOCH3, is easily accomplished using microscale glassware.

Convenient Microscale Synthesis of a Coumarin Laser …

Microscale syntheses of anti-tumour platinum …

The main pedagogical characteristics of this laboratory instructionincluded two aspects to be expected. In terms of pedagogical characteristics:emphasis on students' reflections in between microscale and macroscale,accent on students' introspection in green chemistry and environmentalprotection, as well as emphasis on the significance of multi-styledesign with chemical experiments. In terms of content knowledgeand laboratory technique: comprehending the synthesis and characterizationof AuNPs, proficiency in the technique of microscale chemistry,expertizing in taking UV-visible absorption spectrum and in testingfor the aggregation using liquid balls, as well as understandingin nanoparticles and green chemistry.

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